Massenspektrometrische Untersuchungen von PhthalocyaninenPc—MeXn
Identifieur interne : 000A36 ( Main/Exploration ); précédent : 000A35; suivant : 000A37Massenspektrometrische Untersuchungen von PhthalocyaninenPc—MeXn
Auteurs : RBID : ISTEX:706_1974_Article_BF00907380.pdfAbstract
PhthalocyaninesPc−Me(III)X andPc−Me(V)X3 were obtained by reacting anhydrous metal halides with phthalodinitrile and di-lithium-phthalocyanine, resp. A phthalocyanine containing niobium(V) was prepared for the first time. Mass spectrometric investigation of the products formed show the molecular ion in the case of chloro-aluminum-, chloro-indium- and tribromo-niobium-phthalocyanine. The mass spectra of chloro-scandium-, chloro-yttrium- and tribromo-tantalum-phthalocyanine showed neither peaks of the molecular mass nor metal containing fragments of the phthalocyanine structure. Mass spectrometric results seem to depend critically on the purity of the compounds employed.
DOI: 10.1007/BF00907380
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Maresch</name><affiliation wicri:level="1"><mods:affiliation>Instituten für Allgemeine Chemie und für Anorganische Chemie der Technischen Hochschule Wien, Lehárgasse 4, A-1060, Wien, Österreich</mods:affiliation><country xml:lang="fr">Autriche</country><wicri:regionArea>Instituten für Allgemeine Chemie und für Anorganische Chemie der Technischen Hochschule Wien, Lehárgasse 4, A-1060, Wien</wicri:regionArea><wicri:noRegion>Wien</wicri:noRegion></affiliation><affiliation wicri:level="1"><mods:affiliation>Anorganisch-Chemischen Institut der Universität Göttingen, Bundesrepublik Deutschland</mods:affiliation><country xml:lang="fr">Allemagne</country><wicri:regionArea>Anorganisch-Chemischen Institut der Universität Göttingen</wicri:regionArea></affiliation></author><author><name>A. Meller</name><affiliation wicri:level="1"><mods:affiliation>Instituten für Allgemeine Chemie und für Anorganische Chemie der Technischen Hochschule Wien, Lehárgasse 4, A-1060, Wien, Österreich</mods:affiliation><country xml:lang="fr">Autriche</country><wicri:regionArea>Instituten für Allgemeine Chemie und für Anorganische Chemie der Technischen Hochschule Wien, Lehárgasse 4, A-1060, Wien</wicri:regionArea><wicri:noRegion>Wien</wicri:noRegion></affiliation><affiliation wicri:level="1"><mods:affiliation>Anorganisch-Chemischen Institut der Universität Göttingen, Bundesrepublik Deutschland</mods:affiliation><country xml:lang="fr">Allemagne</country><wicri:regionArea>Anorganisch-Chemischen Institut der Universität Göttingen</wicri:regionArea></affiliation></author></titleStmt><publicationStmt><idno type="RBID">ISTEX:706_1974_Article_BF00907380.pdf</idno><date when="1974">1974</date><idno type="doi">10.1007/BF00907380</idno><idno type="wicri:Area/Main/Corpus">000573</idno><idno type="wicri:Area/Main/Curation">000573</idno><idno type="wicri:Area/Main/Exploration">000A36</idno></publicationStmt></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="eng">PhthalocyaninesPc−Me(III)X andPc−Me(V)X3 were obtained by reacting anhydrous metal halides with phthalodinitrile and di-lithium-phthalocyanine, resp. A phthalocyanine containing niobium(V) was prepared for the first time. Mass spectrometric investigation of the products formed show the molecular ion in the case of chloro-aluminum-, chloro-indium- and tribromo-niobium-phthalocyanine. The mass spectra of chloro-scandium-, chloro-yttrium- and tribromo-tantalum-phthalocyanine showed neither peaks of the molecular mass nor metal containing fragments of the phthalocyanine structure. Mass spectrometric results seem to depend critically on the purity of the compounds employed.</div></front></TEI><mods xsi:schemaLocation="http://www.loc.gov/mods/v3 file:///applis/istex/home/loadistex/home/etc/xsd/mods.xsd" version="3.4" istexId="636704407ad079baed421660119bbe1ee1508deb"><titleInfo lang="ger"><title>Massenspektrometrische Untersuchungen von PhthalocyaninenPc—MeXn</title></titleInfo><titleInfo lang="eng"><title>Mass spectrometric investigation of phthalocyanines Pc−MeXn</title></titleInfo><name type="personal"><namePart type="termsOfAddress">Dr.</namePart><namePart type="given">K.</namePart><namePart type="family">Varmuza</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Instituten für Allgemeine Chemie und für Anorganische Chemie der Technischen Hochschule Wien, Lehárgasse 4, A-1060, Wien, Österreich</affiliation><affiliation>Anorganisch-Chemischen Institut der Universität Göttingen, Bundesrepublik Deutschland</affiliation></name><name type="personal"><namePart type="termsOfAddress"></namePart><namePart type="given">G.</namePart><namePart type="family">Maresch</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Instituten für Allgemeine Chemie und für Anorganische Chemie der Technischen Hochschule Wien, Lehárgasse 4, A-1060, Wien, Österreich</affiliation><affiliation>Anorganisch-Chemischen Institut der Universität Göttingen, Bundesrepublik Deutschland</affiliation></name><name type="personal"><namePart type="termsOfAddress"></namePart><namePart type="given">A.</namePart><namePart type="family">Meller</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Instituten für Allgemeine Chemie und für Anorganische Chemie der Technischen Hochschule Wien, Lehárgasse 4, A-1060, Wien, Österreich</affiliation><affiliation>Anorganisch-Chemischen Institut der Universität Göttingen, Bundesrepublik Deutschland</affiliation></name><typeOfResource>text</typeOfResource><genre>Organische Chemie und Biochemie</genre><genre>Original Paper</genre><originInfo><publisher>Springer-Verlag, Vienna</publisher><dateCreated encoding="w3cdtf">1973-12-20</dateCreated><dateValid encoding="w3cdtf">2004-12-15</dateValid><copyrightDate encoding="w3cdtf">1974</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">ger</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="eng">PhthalocyaninesPc−Me(III)X andPc−Me(V)X3 were obtained by reacting anhydrous metal halides with phthalodinitrile and di-lithium-phthalocyanine, resp. A phthalocyanine containing niobium(V) was prepared for the first time. Mass spectrometric investigation of the products formed show the molecular ion in the case of chloro-aluminum-, chloro-indium- and tribromo-niobium-phthalocyanine. The mass spectra of chloro-scandium-, chloro-yttrium- and tribromo-tantalum-phthalocyanine showed neither peaks of the molecular mass nor metal containing fragments of the phthalocyanine structure. Mass spectrometric results seem to depend critically on the purity of the compounds employed.</abstract><relatedItem type="series"><titleInfo type="abbreviated"><title>Monatshefte für Chemie</title></titleInfo><titleInfo><title>Monatshefte für Chemie / Chemical Monthly</title><partNumber>Year: 1974</partNumber><partNumber>Volume: 105</partNumber><partNumber>Number: 2</partNumber></titleInfo><genre>Archive Journal</genre><originInfo><dateIssued encoding="w3cdtf">1974-03-01</dateIssued><copyrightDate encoding="w3cdtf">1974</copyrightDate></originInfo><subject usage="primary"><topic>Chemistry</topic><topic>Chemistry/Food Science, general</topic><topic>Analytical Chemistry</topic><topic>Inorganic Chemistry</topic><topic>Organic Chemistry</topic><topic>Physical Chemistry</topic><topic>Theoretical and Computational Chemistry</topic></subject><identifier type="issn">0026-9247</identifier><identifier type="issn">Electronic: 1434-4475</identifier><identifier type="matrixNumber">706</identifier><identifier type="local">IssueArticleCount: 27</identifier><recordInfo><recordOrigin>Springer-Verlag, 1974</recordOrigin></recordInfo></relatedItem><identifier type="doi">10.1007/BF00907380</identifier><identifier type="matrixNumber">Art12</identifier><identifier type="local">BF00907380</identifier><accessCondition type="use and reproduction">MetadataGrant: OpenAccess</accessCondition><accessCondition type="use and reproduction">AbstractGrant: OpenAccess</accessCondition><accessCondition type="restriction on access">BodyPDFGrant: Restricted</accessCondition><accessCondition type="restriction on access">BodyHTMLGrant: Restricted</accessCondition><accessCondition type="restriction on access">BibliographyGrant: Restricted</accessCondition><accessCondition type="restriction on access">ESMGrant: Restricted</accessCondition><part><extent unit="pages"><start>327</start><end>333</end></extent></part><recordInfo><recordOrigin>Springer-Verlag, 1974</recordOrigin><recordIdentifier>706_1974_Article_BF00907380.pdf</recordIdentifier></recordInfo></mods></record>Pour manipuler ce document sous Unix (Dilib)
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